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12%Guo S, Feng B, Zhang H (2011) Simultaneous determination of trace arsenic and antimony in Fomes Officinalis Ames with hydride generation atomic fluorescence spectrometry. J Fluoresc 21:1281–1284. CAS Article Google Scholar 21.
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The analytical results of arsenic and antimony in spring waters at several sites in Japan by this method were in good agreement with those obtained by the hydride generation AAS. KW - XRF analysis of arsenic and antimony. KW - coprecipitation of zirconium hydroxide. KW - determination of arsenic and antimony in spring water
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1. Ann Occup Hyg. 1988;32(3):385-97. Determination of hydrides of arsenic, antimony and tin in workplace air. Pedersen B. PMID: 3202549 [PubMed - indexed for MEDLINE]
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@article{osti_5001009, title = {Determination of arsenic, antimony, and selenium in coal by atomic absorption spectrometry with a graphite tube atomizer}, author = {Aruscavage, P}, abstractNote = {Submicrogram quantities of antimony, arsenic, and selenium in coal samples are determined by an atomic absorption procedure using an electrically heated graphite atomizer.
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Determination of oxoanions and water-soluble species of arsenic, selenium, antimony, vanadium, and chromium eluted in water from airborne fine particles (PM 2.5): effect of acid and transition metal content of particles on heavy metal elution†
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Research | Articles Development and Application of a Robust Speciation Method for Determination of Six Arsenic Compounds Present in Human Urine Lisa S. Milstein,1 Amal Essader,1 Edo D. Pellizzari,1 Reshan A. Fernando,1 James H. Raymer,1 Keith E. Levine,1 and Olujide Akinbo2 1Research Triangle Institute, Research Triangle Park, North Carolina, USA; 2Butler University, Department of Chemistry ...
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The water samples containing 0.30 mg L.-1 of antimony and 2.0 mg L-l of mercury show absorbance peaks at 510 nm (average absorbance .007) and 425 nm (average absorbance .005) resoectively and thus these ions are expected to interfere positively in the determination of arsenic …
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ISO 17378-1:2014 specifies a method for the determination of arsenic and antimony. The method is applicable to drinking water, surface water, ground water and rain water. The linear application range of ISO 17378-1:2014 is from 0,02 µg/l to 100 µg/l.
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The analytical method is validated for the determination of arsenic and its compounds in the air of workplaces averaged over the sampling period after personal or stationary sampling. Sampling is performed by drawing a defined volume of air through a membrane filter located in the sampling head of a total dust sampling system ( G esamt- S taub ...
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The methods used for separation of arsenic from the solution or for the concentration of arsenic are: distillation after reduction to arsenic hydride, extraction of halogen-ides by CCl 4 from an acidic environment and extraction of the diethyldithiocarbaminate complex with As (III) [7]. Spectrophotometric Methods for Determination of Antimony
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Orvini, Edoardo., Gills, Thomas E., LaFleur, Philip D. (1974) Method for determination of selenium, arsenic, zinc, cadmium, and mercury in environmental matrices by ...
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the determination of arsenic. Spectrochemical analyses by Scribner (73) showed no antimony in one sample each of Florida land pebble and Tennessee brown rock; so far as the authors know, these are the only tests that have been made for antimony in natural phosphates. According to Byers and Robinson," small quantities of antimony do
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THE DETERMINATION OF ARSENIC, ANTIMONY, SELENIUM AND TELLURIUM IN ENVIRONMENTAL WATER SAMPLES BY FLAMELESS ATOMIC ABSORPTION By G. C. KUNSELMAN AND E. A. HUFF U.S. ENVIRONMENTAL PROTECTION AGENCY CENTRAL REGIONAL LABORATORY 1819 WEST PERSHING ROAD CHICAGO, ILLINOIS 60609 Ouly 1, 1975 ----- BRIEF Total arsenic, antimony…
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A method is described for the determination of ultramicro quantities of arsenic and antimony in pure platinum. In order to avoid self-shielding differences between sampies and standards during neutron irradiation, comparators were prepared by the addition of very small known amounts of arsenic and antimony to analytical samples.
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The determination of the chemical species of the "hydribe elements" (arsenic, antimony, tin and germanium) in seawater: Methodogy and results. In: Wong CS, Boyle E, Bruland
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Determination of Arsenic and Antimony Together: Instead of separating arsenic from antimony in the hydrochloric-tartaric acid solution which was finally obtained, dilute the solution to four times its volume; pass sulphuretted hydrogen to saturation; filter the combined sulphides on a 4 cm. filter (weighed and dried in weigh-bottle at 110° C.); wash with water, absolute alcohol, carbon ...
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Antimony, arsenic, bismuth and copper have been selected as major electrolyte constituents. For these elements pr … Determination of antimony, arsenic, bismuth and copper by inductively coupled plasma atomic emission spectrometry in the electrorefining of copper
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and determination of arsenic, antimony and tin, as described in sec tion II, 4 and 5. 2. IN TIN-BASE ALLOYS (a) PREPARATION OF THE SOLUTION The following procedure is designed for the determination of arsenic, antimony, and tin in tin-antimony alloys which contain little or no lead. The sample taken should not contain more than 100 mg of
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Slurry-based procedures for the rapid determination of arsenic and antimony in soil and sediment samples by graphite furnace atomic absorption spectrometry are discussed. For the determination of arsenic, the samples are suspended in a solution containing dilute hydrofluoric acid. Sodium hydrogen carbonate is added and aliquots are introduced into the graphite furnace.
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： The antimony slab and antimonous oxide samples were dissolved by sulfuric acid and hydrochloric acid,respectively.The Sb3+ in solution was precipitated with sodium hydroxide to separate trace arsenic from matrix antimony.The thiourea-ascorbic acid was added to reduce As5+ to As3+.Then,the arsenic in antimony slab and antimonous oxide was determined by atomic …
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and ICP for determination of arsenic, FAAS, GF AAS, HGAAS for determination of antimony, the spectrophoto- metric method with 2,3-diaminenaphthalene, fluorimetric
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A method for the determination of arsenic, bismuth, germanium, lead, antimony, selenium, tin and tellurium by means of hydride generation is described. The hydrides are generated by adding the acidified sample to dilute (1 per cent. /) sodium borohydride solution. The …
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Arsenic is BAD! DETERMINATION OF ARSENIC WITH POTASSIUM PERMANGANATE. OBJECTIVE: 1. The student will use the strong oxidant KMnO 4 as a titrant. 2. This is a self-indicating titrant. 3. The standard and the unknown are treated the same in this method. 4. The student will use a …
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Methods for the simultaneous determination and speciation of arsenic, selenium and antimony in complex matrices involving inductively coupled plasma optical emission spectrometry (ICP-OES), and inductively coupled plasma mass spectrometry (ICP-MS) coupled with high performance liquid chromatography (HPLC) were developed and successfully applied to the analyses of various types of …
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separation and determination of tin, arsenic, and antimony. The elements all of them give to their alloys with many of the other metals characteristic properties which tend to make them much used, and thus their determination becomes important. As is well known tin …
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HAGEDORN Separationand DeterminationofTin, Arsenic&Antimony Chemistry 192 »•«>•••,»a" OK ' tLt. 3HlltAJii'
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The precision of the determination of the elements in two reference materials (a = 0.05) Volume of extract No. of Material used, ml measurements Element x + (sc,)l$ ppm 1 0.5 5 As 63.5 f 2.9 Sb 115.9 f 1.8 Sn 71.1 f 5.8 2 0.2 5 As 201.5 + 8.2 Sb 214.5 k 5.7 Sn 512 k 38 Determination of arsenic, antimony and tin 1095 Table 8.
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ANTIMONY AND ARSENIC (ATOMIC ABSORPTION, BOROHYDRIDE REDUCTION) 1.0 SCOPE AND APPLICATION 1.1 Method 7062 is an atomic absorption procedure for determining 1 µg/L to 400 µg/L concentrations of antimony and arsenic in wastes, mobility procedure extracts, soils, and ground water. Method 7062 is approved for sample matrices
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The presence of a small amount of tungsten in the filtrate (up to 150 mg/mL) causes spectral interference, which deteriorates the accuracy of the ICP–AES determination of arsenic and antimony; the concentration of arsenic and antimony is higher than that added (see Fig. 4, …
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Total sedimentary arsenic and antimony were determined using the method of Cutter et al. (1991), while the 2 M HC1 leach technique given by Andreae and Froelich (1984) was used to quantify sedimentary arsenic and antimony speciation. DISCUSSION Antimony, arsenic, and selenium have perhaps the most diverse chemistries of the metalloids.
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Arsenic and Antimony in Converter Copper. Treat 10 g. of the sample in a No. 5 beaker with 30 cc. of sulphuric acid, 20 cc. of nitric acid, and about 50 cc. of water. When solution is complete, heat to boiling to drive off all red fumes, add water to fill beaker about two-thirds and electrolyze about 2.5 hr. at 4 amperes.
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Determination of arsenic and antimony 17378 2013 Water quality .,,,。 >> ISO_DIS 09Wrought aluminium and aluminium alloys. Sheets,strips and plates.
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